ft-nir (2)

13707404294?profile=RESIZE_400xIn this study (purchase required), Fourier transform near-infrared spectroscopy (FT-NIRS) was combined with two distinct machine learning algorithms to detect and quantify the peanut adulteration rate (%) in ground hazelnut.

Ground hazelnut samples were mixed with various levels of peanut content (0–50%). The spectral data were collected in the wavelength (λ) range of 4000–10000 cm−1. Feature selection was carried out using the Lasso and Elastic Net algorithms to determine and eliminate unnecessary spectral variables and improve the accuracy of prediction. The Lasso model was found to be more accurate compared to the Elastic Net model for the same λ value (0.001). The authors report that the prediction accuracy indicator values improved as λ values decreased. Cross-validation confirmed the robustness of the Lasso model, indicating it is highly generalisable.

The authors conclude that FT-NIRS, supported by ML-based feature selection and modelling, provides an efficient, fast and non-destructive approach for the detection and quantification of hazelnut adulteration with ground peanut. This approach offers a rapid, waste-free, and eco-friendly solution to food adulteration detection, aligning with sustainable production principles by minimising sample preparation and resource consumption in the frame of greener analytical workflows.

Photo by David Gabrielyan on Unsplash

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12992338473?profile=RESIZE_400xThis Masters’ degree project developed a predictive algorithm to categorize butter, butter spreads, and margarine/vegetable oil spreads according to their fatty acid profile, moisture, and total fat content based on the spectra collected by using handheld FT-NIR and portable FT-MIR devices. FT-NIR infrared and FT-MIR performances were similar, with a strong correlation (Rep >0.94) and low standard error of prediction for different analyzed parameters. SIMCA classification model based on FT-NIR and FT-MIR spectra effectively differentiated between butter, butter spread, and margarine/vegetable oil spreads.

The results were benchmarked against “classical” analysis.  Moisture and total fat content were determined using reference methods AOAC 920.116 and AOAC 938.06-1938, respectively. FA profile was determined using Gas Chromatography with flame ionization detector (GC-FID) (AOAC 996.06, 1996.). The FA profile showed that butter-containing products distinguished from margarine/vegetable oil spreads based on the presence of trans fats (TFA) (C18:1t) and butyric acid (C4:0).

The author concludes that portable FT-MIR and handheld FT-NIR technologies offer real-time and in situ analysis capabilities, enabling the dairy industry and regulatory agencies to make actionable decisions regarding FA, moisture, and total fat content and for nutrition, authentication, claims, and labeling purposes of these products.

The abstract and author contact details are available here.  The full text is being withheld until May 2026 at the author’s request. For an overview of FT-NIR see FAN's analytical techniques explainer for spectroscopy.

Photo by Sorin Gheorghita on Unsplash

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